HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86631064, compound → (Cis)-[4-chloro-2-[[2,3-dimethyl-4-(phenylacetyl)-1-piperazinyl]methyl]phenoxy]-acetic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86631064 | HCID 86631064 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | (Cis)-[4-chloro-2-[[2,3-dimethyl-4-(phenylacetyl)-1-piperazinyl]methyl]phenoxy]-acetic Acid | HCID 67131752 | — |
Reaction Steps
The product from example 71 part b) treated with TFA (10 ml) for 16 h. Concentration in vacuo and purification by RPHPLC gave the title product as a white foam (39 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08524715B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-be08dd6f876d4af3aa0f440e528cfbe8 |
| Source note | uspto-grants-2013_09 |