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HRID38282

反应详情

EQUATION

反应方程式

HRID 38282 的结构方程式

REACTANTS

反应物

1
结构：C[C@@H]1[C@H](C)N(Cc2cc(Cl)ccc2OCC(=O)OC(C)(C)C)CCN1C(=O)Cc1ccccc1
HCID86631064

未命名化合物

PRODUCTS

生成物

1
结构：C[C@@H]1[C@H](C)N(Cc2cc(Cl)ccc2OCC(=O)O)CCN1C(=O)Cc1ccccc1
HCID67131752

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O=C(O)C(F)(F)F
溶剂HCID6422

未命名化合物

PROCEDURE

实验过程

The product from example 71 part b) treated with TFA (10 ml) for 16 h. Concentration in vacuo and purification by RPHPLC gave the title product as a white foam (39 mg).

WORKUP

后处理

  1. concentrationConcentration
  2. customin vacuo and purification by RPHPLC