Resorcinol → 3-(Pentyloxy)phenol

HRID 382907Notes

Reaction equation

[C:1]1([CH:8]=[CH:7][CH:6]=[C:4]([OH:5])[CH:3]=1)[OH:2].[CH2:9](Br)[CH2:10][CH2:11][CH2:12][CH3:13]>>[CH2:9]([O:2][C:1]1[CH:3]=[C:4]([OH:5])[CH:6]=[CH:7][CH:8]=1)[CH2:10][CH2:11][CH2:12][CH3:13]

Participants

Reactant 2

HCID 5054Resorcinol

HCID 80571-Bromopentane

Product 1

HCID 156922293-(Pentyloxy)phenolYield 39.9%

Procedure

Prepared according to the method described in Example A above from resorcinol (55 g; 0.5 mol) and n-pentylbromide (83.1 g; 0.55 mol) to yield 36.0 g (40%) of the title compound as an oil (92% purity). bp 128-131° C. (5 mm Hg) MW=180 (GC-MS)

Workup

customPrepared

Sources & evidence

ORD record: ord-7ac5d3555f2f45dda9dc94a720747181
Source dataset: uspto-grants-2001_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06310252B1

Reaction notes

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