HuagongsheHuagongshe Chemistry Print Report · For research reference only
Citric Acid → HCID 18361599, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Citric Acid | HCID 311 | — |
| Reactant | HCID 9823548 | HCID 9823548 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18361599 | HCID 18361599 | 97.5% |
Reaction Steps
To a solution of (−)-6-(4-biphenylyl)methoxy-2-[2-(N,N-dimethylamino)ethyl]tetralin (1.3 g) in methanol (10 ml) was added a solution of citric acid (0.65 g) in methanol (10 ml) and the resulting precipitated salt was collected by filtration and washed with methanol, ethyl acetate, and diethyl ether to obtain the titled compound (1.9 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06310107B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-9a75b74f3aad4090b38347173184bd58 |
| Source note | uspto-grants-2001_10 |