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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 382971Generated: October 29, 2026

Citric Acid → HCID 18361599, compound

https://huagongshe.com/reaction/382971

Reaction equation

Participants

RoleNameHCIDCharge
ReactantCitric AcidHCID 311—
ReactantHCID 9823548HCID 9823548—
SolventMethanolHCID 887—
ProductHCID 18361599HCID 1836159997.5%

Reaction Steps

To a solution of (−)-6-(4-biphenylyl)methoxy-2-[2-(N,N-dimethylamino)ethyl]tetralin (1.3 g) in methanol (10 ml) was added a solution of citric acid (0.65 g) in methanol (10 ml) and the resulting precipitated salt was collected by filtration and washed with methanol, ethyl acetate, and diethyl ether to obtain the titled compound (1.9 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06310107B1
Source datasetuspto-grants-2001_10
ORD IDord-9a75b74f3aad4090b38347173184bd58
Source noteuspto-grants-2001_10