Hydrochloric Acid → HCID 18361502, compound
Reaction equation
[C:1]1([C:24]2[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=2)[CH:6]=[CH:5][C:4]([CH2:7][O:8][C:9]2[CH:10]=[C:11]3[C:16](=[CH:17][CH:18]=2)[CH2:15][CH:14]([CH2:19][CH2:20][NH:21][CH2:22][CH3:23])[CH2:13][CH2:12]3)=[CH:3][CH:2]=1.[ClH:30]>>[ClH:30].[C:1]1([C:24]2[CH:25]=[CH:26][CH:27]=[CH:28][CH:29]=2)[CH:2]=[CH:3][C:4]([CH2:7][O:8][C:9]2[CH:10]=[C:11]3[C:16](=[CH:17][CH:18]=2)[CH2:15][CH:14]([CH2:19][CH2:20][NH:21][CH2:22][CH3:23])[CH2:13][CH2:12]3)=[CH:5][CH:6]=1Participants
3
Procedure
6-(4-Biphenylyl)methoxy-2-[2-(N-ethylamino)ethyl]tetralin (1.009 g) was converted into its hydrochloride. The hydrochloride was washed with methanol, ethyl acetate, and diethyl ether to obtain the titled compound (810 mg).
Workup
- washThe hydrochloride was washed with methanol, ethyl acetate, and diethyl ether
Sources & evidence
- ORD record
- ord-9bdb37f3d243425ab6c529c2c376b678
- Source dataset
- uspto-grants-2001_10
- Patent number
- US06310107B1
Reaction notes
Loading…