HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cesium carbonate → HCID 18429323, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | 1-Acetoxy-2-bromoethane | HCID 13564 | — |
| Reactant | HCID 18429155 | HCID 18429155 | — |
| Product | HCID 18429323 | HCID 18429323 | — |
Reaction Steps
5-(2-Acetoxypropionylamino)-3-acetoxymethyl-N-(1,3,4-triacetoxybut-2-yl)-2,4,6-triiodobenzamide (Example 37a) was N-alkylated using 2-bromoethyl acetate and cesium carbonate according to the procedure in Example 30a. The yield of isolated product was 82.4%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06310243B1 |
| Source dataset | uspto-grants-2001_10 |
| ORD ID | ord-db2cc77ca9b648b08a81ba0e7b2e6f5b |
| Source note | uspto-grants-2001_10 |