Phenethylamine → HCID 18361059, compound

Participants

Reaction Steps

To a stirred solution at ambient temperature of phenethylamine (200 mg, 1.65 mmol) in CH2Cl2 (2 mL) was added triethylamine (0.35 mL, 2.48 mmol) and butanesulfonyl chloride (0.24 mL, 1.82 mmol). After 4 hours of stirring at ambient temperature, the reaction was diluted with EtOAc and washed with water, 1.0M NaHCO3, and brine. Organic layer dried with Na2SO4, filtered, and concentrated in vacuo.

Provenance & Evidence