HRID383231

反应详情

EQUATION

反应方程式

HRID 383231 的结构方程式

PROCEDURE

实验过程

4′,7-Dihydroxyisoflav-3-ene (507 mg, 2.11 mmol) was dissolved in ethanol (20 ml). Methylamine solution (0.6 ml, 4.82 mmol, 33% wt. in ethanol) was added followed by formaldehyde solution (2 ml, 0.03 mol, 37% wt.). The reaction was stirred at room temperature for 1 day. The white precipitate was collected to afford the title compound (490 mg, 79%).

WORKUP

后处理

  1. customThe white precipitate was collected