HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 25002234, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | HCID 57871385 | HCID 57871385 | — |
| Product | HCID 25002234 | HCID 25002234 | 15% |
Reaction Steps
7-Hydroxy-3′,4′-dimethoxy-8-methylisoflav-3-ene (155 mg, 0.52 mmol) was dissolved in ethanol (2.5 ml). Benzylamine (0.07 ml, 023 mmol) was added followed by formaldehyde solution (0.6 ml, 8.06 mmol, 37% wt.). The reaction was stirred at room temperature for 2 days. The precipitate was collected to afford the title compound (33 mg, 15%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08367659B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-61bfacac83a94dfc9e71fe3181af57f4 |
| Source note | uspto-grants-2013_02 |