HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 25007238, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | m-Toluidine | HCID 7934 | — |
| Reactant | Phenoxodiol | HCID 219100 | — |
| Product | HCID 25007238 | HCID 25007238 | 48% |
Reaction Steps
4′,7-Dihydroxyisoflav-3-ene (522 mg, 2.17 mmol) was dissolved in ethanol (8 ml). m-Toluidine (0.3 ml, 2.77 mmol) and formaldehyde solution (2 ml, 0.03 mol, 37% wt.) were added and the reaction stirred at room temperature for 3 days. The resulting precipitate was collected to afford the title compound (386 mg, 48%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08367659B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-cec70e4f00ad450e972f95aacc4aaabf |
| Source note | uspto-grants-2013_02 |