HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 66977868, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Ethyl 7-bromoheptanoate | HCID 122490 | — |
| Reactant | HCID 66977641 | HCID 66977641 | — |
| Reactant | HCID 66977722 | HCID 66977722 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 66977868 | HCID 66977868 | 27% |
| Product | HCID 67146620 | HCID 67146620 | 16% |
Reaction Steps
The title compound 0115-5 (110 mg, 27%) and 0116-5 (60 mg, 16%) were prepared from 0114 (280 mg, 0.55 mmol) , ethyl 7-bromoheptanoate (133 mg, 0.65 mmol) and potassium carbonate (152 mg, 1.10 mmol) in acetonitrile (25 mL) using a procedure similar to that described for compound 0115-3 and compound 0116-3 (Example 1):
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08367663B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-360108300bf6452d9f8e4c75660e8a46 |
| Source note | uspto-grants-2013_02 |