HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 383627Generated: November 2, 2026
Methanol → Methyl 3-(6-oxo-1,6-dihydropyridazin-3-yl)benzoate
https://huagongshe.com/reaction/383627
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3-(6-Oxo-1,6-dihydropyridazin-3-yl)benzoic acid | HCID 59406771 | — |
| Product | Methyl 3-(6-oxo-1,6-dihydropyridazin-3-yl)benzoate | HCID 59406653 | — |
Reaction Steps
12.3 g (57 mmol) of 3-(6-oxo-1,6-dihydropyridazin-3-yl)benzoic acid are dissolved in 240 ml of methanol, and 30 ml of thionyl chloride are added. The reaction mixture is stirred at 70° C. for 24 h. The reaction solution is evaporated, and the residue is digested with diethyl ether, and the residue is dried in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08367668B2 |
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| Source dataset | uspto-grants-2013_02 |
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| ORD ID | ord-97d14e8844a941e784fd506b6f891523 |
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| Source note | uspto-grants-2013_02 |
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