HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 59807763, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 59808009 | HCID 59808009 | — |
| Product | HCID 59807763 | HCID 59807763 | — |
Reaction Steps
In a manner similar to that described for Examples 1B-C, the title compound was prepared from 2-[3-(4-methanesulfonyl-phenylcarbamoyl)-2,5-dimethyl-pyrrol-1-yl]-benzoic acid and ammonia. 1H-NMR (DMSO-d6): δ 9.82 (1H, s), 8.08 (2H, d, J=9.1), 7.90 (2H, d, J=9.1), 7.67 (4H, m), 7.39 (1H, s). 7.34 (1H, m), 6.63 (1H, s), 3.23 (3H, s), 2.27 (3H, s), 2.00 (3H, s); MS (ESI): 412 (MH+). C. In a manner similar to that described for Example 21B, the following compounds were prepared from the appropriate amines:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08367667B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-6be91103895a470f9b80f5bf5a8e42c1 |
| Source note | uspto-grants-2013_02 |