Hydrochloric Acid → HCID 86661359, compound

Participants

Reaction Steps

To the solution of 1-tert-butyl 3-methyl trans-5-azidopiperidine-1,3-dicarboxylate (343.0 mg) in MeOH (1 ml) was added 10% solution of HCl in MeOH (15 ml). After stirring for 30 minutes at room temperature, the mixture was concentrated to give the crude methyl cis-5-azidopiperidine-3-carboxylate hydrochloride (120.3 mg) as a pale brown solid.

Provenance & Evidence