HRID383824

反应详情

EQUATION

反应方程式

HRID 383824 的结构方程式

PROCEDURE

实验过程

The compound was prepared according to the procedure disclosed in Example 1a starting from benzylpiperazine (16.1 mL, 92.6 mmol) and 7-bromo-benzofuran-2-carboxylic acid ethyl ester (16.6 g, 61.7 mmol). The product was purified by flash chromatography (SiO2; hexane/EtOAc, gradient 0-50%). Yield: 14 g (63%).

WORKUP

后处理

  1. customThe compound was prepared
  2. customThe product was purified by flash chromatography (SiO2; hexane/EtOAc, gradient 0-50%)