HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen chloride-ethyl acetate → HCID 68430374, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Reactant | HCID 86649436 | HCID 86649436 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 68430374 | HCID 68430374 | 100% |
Reaction Steps
A 4 N-hydrochloric acid-ethyl acetate solution (8.1 mL) was added to a chloroform (10 mL) solution of the compound (1.26 g, 3.24 mmol) synthesized in (3), and the mixture was stirred at room temperature for 13 hours. The reaction mixture was then concentrated under reduced pressure to obtain the title compound (1.15 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08367698B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-94e93848fc4645118f2fbea65ba3a85b |
| Source note | uspto-grants-2013_02 |