HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 4-(2-chloroethyl)hexahydro-1-(phenylmethyl)-1H-azepine-4-carboxylate → HCID 86641067, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 4-(2-chloroethyl)hexahydro-1-(phenylmethyl)-1H-azepine-4-carboxylate | HCID 59291310 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 86641067 | HCID 86641067 | 100% |
Reaction Steps
A solution of ethyl 1-benzyl-4-(2-chloroethyl)azepane-4-carboxylate (4.1 g) in MeCN (200 mL) was stirred at 40° C. for 10 hours. The reaction mixture was concentrated under reduced pressure to obtain 1-benzyl-5-(ethoxycarbonyl)-1-azoniabicyclo[3.2.2]nonane chloride (4.1 g) as a colorless oily substance.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08367696B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-61abf6fcafcb4998ac791364c8ce26fd |
| Source note | uspto-grants-2013_02 |