HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86641942, compound → HCID 67272423, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86641942 | HCID 86641942 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67272423 | HCID 67272423 | — |
Reaction Steps
To a solution of (6-chloro-3-phenoxypyridin-2-yl)methanol (88 mg) in ethanol (1.5 ml), 10 mg of 10% palladium-carbon catalyst was added, and the reaction solution was stirred for 20 hours under hydrogen atmosphere. The catalyst was filtered off through Celite, and the filtrate was distilled off under reduced pressure to afford the title compound as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08367708B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-bd62ea0b8b5c446fa104de0383a94650 |
| Source note | uspto-grants-2013_02 |