HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86641944, compound → HCID 178515868, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86641944 | HCID 86641944 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 178515868 | HCID 178515868 | — |
Reaction Steps
To a solution of N-hydroxy-3-oxo-4-(4-((2-phenoxybenzyl)oxy)phenyl)butanamide (17.2 mg) in acetic acid (0.2 ml), 0.05 ml of concentrated hydrochloric acid was added, and the reaction solution was stirred overnight at room temperature. The solvent was distilled off under reduced pressure, and the residue obtained was purified by preparative thin layer chromatography (Kieselgel™ 60 F254, Art5744, made by Merck & Co., hexane/ethyl acetate (1:1) to afford the title compound as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08367708B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-8537372c91304d5881a9630d28a0b30f |
| Source note | uspto-grants-2013_02 |