HRID384262

反应详情

EQUATION

反应方程式

HRID 384262 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a solution of N-(5-nitro-2-(2-(pyrrolidin-1-yl)ethoxy)phenyl)acetamide (430 mg) in EtOH (10 mL) was added Pd/C (200 mg) and was charged with H2 (1 atm). After stirring for 3 h, Pd/C was removed by filtration and the filtrate was concentrated to give N-(5-amino-2-(2-(pyrrolidin-1-yl)ethoxy)phenyl)acetamide (380 mg).

WORKUP

后处理

  1. additionwas charged with H2 (1 atm)
  2. customPd/C was removed by filtration
  3. concentrationthe filtrate was concentrated