HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59526915, compound → HCID 19733794, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59526915 | HCID 59526915 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 19733794 | HCID 19733794 | 27.8% |
Reaction Steps
To a solution of {[4-(2,2-dimethylpropoxy)butoxy]methyl}benzene (1.50 g) in acetic acid (30 mL) was added 10% palladium-activated carbon (500 mg), followed by stirring under hydrogen atmosphere for 3 hours. The catalyst was removed by filtration, and the solvent was evaporated under reduced pressure to obtain 4-(2,2-dimethylpropoxy)butan-1-ol (267 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08367702B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-c7ea222b1c7a4e3cb94b862412a22ff3 |
| Source note | uspto-grants-2013_02 |