HRID384583

反应详情

EQUATION

反应方程式

HRID 384583 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
60 °C

PROCEDURE

实验过程

In a 200-liter reactor equipped with a stirrer, a cooling apparatus, a condenser and a monomer supplying tube, 5 parts by weight of butylacrylate, 15 parts by weight of styrene, 0.2 parts by weight of triallyl isocyanurate, 140 parts by weight of ion-exchanged water and 1.0 parts by weight of potassium rosinate are added and mixed. The temperature is raised to 60° C. with stirring. After 10 minutes from the time of reaching 60° C., 0.25 parts by weight of potassium persulfate dissolved in deionized water is added thereto to initiate polymerization. The temperature of the reactor is maintained at 70° C. for 60 minutes. The polymerization is carried out at 70° C. for an additional 30 minutes to give an inner core of butylacrylate-styrene copolymer.

WORKUP

后处理

  1. customIn a 200-liter reactor equipped with a stirrer
  2. additionmixed
  3. additionis added
  4. custompolymerization
  5. temperatureThe temperature of the reactor is maintained at 70° C. for 60 minutes
  6. waitThe polymerization is carried out at 70° C. for an additional 30 minutes