HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-Aminopropyl)triethoxysilane → HCID 123912826, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-Aminopropyl)triethoxysilane | HCID 13521 | — |
| Reactant | HCID 86629708 | HCID 86629708 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 123912826 | HCID 123912826 | — |
Reaction Steps
3-Aminopropyltriethoxysilane (22.14 g, 0.100 mol) is added to a solution of 26.03 g (0.100 mol) of 6-(4-methoxy-benzoyl)-7-oxa-bicyclo[4.2.0]octan-8-one in methylene chloride. The reaction mixture is heated at reflux for several hours and monitored by thin layer chromatography. Upon completion of the reaction, solvent is evaporated to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08367743B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-e2c8c5c7d85d49189264da01c1161d4b |
| Source note | uspto-grants-2013_02 |