HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 86668177, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 68108612 | HCID 68108612 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 86668177 | HCID 86668177 | — |
Reaction Steps
To 4-methoxy-3-(pyrrolidine-1-carbonyl)-5-trifluoromethylbenzoic acid (785 mg), toluene (8 mL) and oxalyl chloride (0.64 mL) were added, and then the mixture was stirred at room temperature for 22 hours. The solvent was distilled off under reduced pressure and the obtained product was used for the synthesis of (d).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08367843B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-348a273fc74649e3a137eb1da298f248 |
| Source note | uspto-grants-2013_02 |