反应详情

温度

220 °C

A mixture of 2,11-dimethoxytriphenylene (8.8 g, 30.5 mmol) and pyridine hydrochloride (31.73 g, 274.6 mmol) was heated to 220° C. for 2 hours. The mixture was cooled and water was added. The resulting solid was filtered off, washed with water, and dried under high vacuum. 7.45 g (94%) desired product was obtained.

1. temperatureThe mixture was cooled
2. filtrationThe resulting solid was filtered off
3. washwashed with water
4. customdried under high vacuum