HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 385308Generated: October 29, 2026
Pyridinium chloride → HCID 58220015, compound
https://huagongshe.com/reaction/385308
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Pyridinium chloride | HCID 10176127 | — |
| Reactant | 2,11-Dimethoxytriphenylene | HCID 58220008 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 58220015 | HCID 58220015 | 94% |
Reaction Steps
A mixture of 2,11-dimethoxytriphenylene (8.8 g, 30.5 mmol) and pyridine hydrochloride (31.73 g, 274.6 mmol) was heated to 220° C. for 2 hours. The mixture was cooled and water was added. The resulting solid was filtered off, washed with water, and dried under high vacuum. 7.45 g (94%) desired product was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08367850B2 |
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| Source dataset | uspto-grants-2013_02 |
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| ORD ID | ord-827a02f3eeda472182aa08c63fb60b40 |
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| Source note | uspto-grants-2013_02 |
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