HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-4-chlorophenol → HCID 66850362, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-4-chlorophenol | HCID 5070078 | — |
| Reactant | tert-Butyl 4-chloro-5,6-dihydropyrido(4',3':4,5)thieno(2,3-d)pyrimidine-7(8H)-carboxylate | HCID 49788563 | — |
| Product | HCID 66850362 | HCID 66850362 | — |
Reaction Steps
The title compound was prepared in analogy to Example 65A from tert-butyl 4-chloro-5,8-dihydropyrido[4′,3′:4,5]thieno[2,3-d]pyrimidine-7(6H)-carboxylate from Example 11A (2.16 g, 6.63 mmol) and 3-amino-4-chlorophenol (1.00 g, 6.97 mmol) to yield 2.26 g (87%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08524722B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-a7b81074ba2f433bae78cf4c09923456 |
| Source note | uspto-grants-2013_09 |