HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Bromopyridine-2-carboxylic acid → 6-Bromo-N-methyl-N-[2-(1-methyl-1H-pyrazol-3-yl)ethyl]pyridine-2-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Bromopyridine-2-carboxylic acid | HCID 593919 | — |
| Reactant | N-Methyl-2-(1-methyl-1H-pyrazol-4-yl)ethan-1-amine | HCID 51000371 | — |
| Product | 6-Bromo-N-methyl-N-[2-(1-methyl-1H-pyrazol-3-yl)ethyl]pyridine-2-carboxamide | HCID 59525757 | — |
Reaction Steps
The title compound was prepared as described in Example 283, Step 1 using N-methyl-2-(1-methyl-1H-pyrazol-4-yl)ethanamine (125 mg, 0.90 mmol) and 6-bromopyridine-2-carboxylic acid (150 mg, 0.74 mmol) as starting materials.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08367706B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-fb2fd803312b46e5b8f2a1f3d680b615 |
| Source note | uspto-grants-2013_02 |