HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 86646269, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 59525561 | HCID 59525561 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86646269 | HCID 86646269 | — |
Reaction Steps
To a solution of methyl(acetyloxy)(6-bromopyridin-2-yl)acetate (1.36 g, 4.70 mmol) in THF (20 mL) and MeOH (10 mL) was added aqueous KOH (1.0 M, 9.88 mL, 9.88 mmol). The solution was stirred at room temperature for 2 hours and then the solvent was evaporated to give the title compound as a colorless solid which was carried on without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08367706B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-00236ba7b9904013bf84a9c13c0d6603 |
| Source note | uspto-grants-2013_02 |