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HRID3863

反应详情

EQUATION

反应方程式

HRID 3863 的结构方程式

REACTANTS

反应物

1
结构：CN(C)c1cc([N+](=O)[O-])ccc1C(=O)Nc1nc[nH]c(=O)c1N
HCID135736201

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)c1cc([N+](=O)[O-])ccc1C1=NC2=NC=NC(=O)C2=N1
HCID20153222

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)O
溶剂HCID176

Acetic Acid

C2H4O2

PROCEDURE

实验过程

One gram of 5-amino-4-(2-dimethylamino-4-nitro-benzoylamino)pyrimidin-6-one is refluxed for two hours in 50 ml of glacial acetic acid. The mixture is evaporated to dryness, and the residue is stirred out with ethanol in the warm.

WORKUP

后处理

  1. customThe mixture is evaporated to dryness