HCID 135736201, compound → 8-(2-Dimethylamino-4-nitro-phenyl)purin-6-one

HRID 3863Notes

Reaction equation

HRID 3863 reaction equation
[NH2:1][C:2]1[C:7](=[O:8])[NH:6][CH:5]=[N:4][C:3]=1[NH:9][C:10](=O)[C:11]1[CH:16]=[CH:15][C:14]([N+:17]([O-:19])=[O:18])=[CH:13][C:12]=1[N:20]([CH3:22])[CH3:21]>C(O)(=O)C>[CH3:21][N:20]([CH3:22])[C:12]1[CH:13]=[C:14]([N+:17]([O-:19])=[O:18])[CH:15]=[CH:16][C:11]=1[C:10]1[N:1]=[C:2]2[C:3](=[N:4][CH:5]=[N:6][C:7]2=[O:8])[N:9]=1

Participants

3

Reactant 1

HCID 135736201HCID 135736201, compound

Product 1

HCID 201532228-(2-Dimethylamino-4-nitro-phenyl)purin-6-one

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

One gram of 5-amino-4-(2-dimethylamino-4-nitro-benzoylamino)pyrimidin-6-one is refluxed for two hours in 50 ml of glacial acetic acid. The mixture is evaporated to dryness, and the residue is stirred out with ethanol in the warm.

Workup

  1. customThe mixture is evaporated to dryness

Sources & evidence

ORD record
ord-cd16ce517d74444e9c3738b0eac46728
Source dataset
uspto-grants-1988_02
Patent number
US04722929

Reaction notes

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