HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 135736201, compound → 8-(2-Dimethylamino-4-nitro-phenyl)purin-6-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 135736201 | HCID 135736201 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 8-(2-Dimethylamino-4-nitro-phenyl)purin-6-one | HCID 20153222 | — |
Reaction Steps
One gram of 5-amino-4-(2-dimethylamino-4-nitro-benzoylamino)pyrimidin-6-one is refluxed for two hours in 50 ml of glacial acetic acid. The mixture is evaporated to dryness, and the residue is stirred out with ethanol in the warm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04722929 |
| Source dataset | uspto-grants-1988_02 |
| ORD ID | ord-cd16ce517d74444e9c3738b0eac46728 |
| Source note | uspto-grants-1988_02 |