huagongshe.com
HRID3865

反应详情

EQUATION

反应方程式

HRID 3865 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)OC(C)=O
HCID7918

Acetic anhydride

C4H6O3

结构：CN(C)c1cc(N)ccc1C1=NC2=NC=NC(=O)C2=N1
HCID20153240

未命名化合物

PRODUCTS

生成物

1
结构：CC(=O)Nc1ccc(C2=NC3=NC=NC(=O)C3=N2)c(N(C)C)c1
HCID20153354

未命名化合物

PROCEDURE

实验过程

A quantity of 0.6 gm of 8-(4-amino-2-dimethylamino-phenyl)purin-6-one is heated to 150° C. in 5 ml of acetic anhydride for one hour. The mixture is evaporated to dryness in vacuo and recrystallized from acetone/ether.

WORKUP

后处理

  1. customThe mixture is evaporated to dryness in vacuo
  2. customrecrystallized from acetone/ether