HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → 8-(4-Acetamido-2-dimethylamino-phenyl)-purin-6-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 8-(4-Amino-2-dimethylamino-phenyl)purin-6-one | HCID 20153240 | — |
| Product | 8-(4-Acetamido-2-dimethylamino-phenyl)-purin-6-one | HCID 20153354 | — |
Reaction Steps
A quantity of 0.6 gm of 8-(4-amino-2-dimethylamino-phenyl)purin-6-one is heated to 150° C. in 5 ml of acetic anhydride for one hour. The mixture is evaporated to dryness in vacuo and recrystallized from acetone/ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04722929 |
| Source dataset | uspto-grants-1988_02 |
| ORD ID | ord-639397261a4c4c98b76a12db25b2c876 |
| Source note | uspto-grants-1988_02 |