HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 38661Generated: October 30, 2026
HCID 56646750, compound → 2-(3-([Bis-[(benzyl)oxy]]phosphoryl)oxy-5-methoxyphenyl)-6,7-methylenedioxyquinolin-4-one
https://huagongshe.com/reaction/38661
Participants
| Role | Name | HCID | Charge |
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| Reactant | HCID 56646750 | HCID 56646750 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-(3-([Bis-[(benzyl)oxy]]phosphoryl)oxy-5-methoxyphenyl)-6,7-methylenedioxyquinolin-4-one | HCID 66659199 | 45% |
Reaction Steps
A suspension of 0.92 g (1.11 mmol) of 167 in 100 mL of methanol was stirred at 25° C. for 48 h. The precipitates were collected and purified by column chromatography (SiO2, EtOAc) to give 168.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08524740B2 |
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| Source dataset | uspto-grants-2013_09 |
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| ORD ID | ord-6ff94a40cbe94c12bb7d85c1cae3b3fd |
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| Source note | uspto-grants-2013_09 |
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