HRID38683

反应详情

EQUATION

反应方程式

HRID 38683 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
80 °C

PROCEDURE

实验过程

3-Bromo-4-methoxyphenylacetic acid (4.1 g, 16.7 mmol) in EtOH (100 mL) was treated with concentrated HCl (2 drops) and heated to 80° C. for 3 days. After cooling to room temperature, the mixture was concentrated to give the title compound.

WORKUP

后处理

  1. temperatureAfter cooling to room temperature
  2. concentrationthe mixture was concentrated