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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 387315Generated: October 29, 2026

2,3-Dichloro-5,6-dicyano-1,4-benzoquinone → HCID 59332625, compound

https://huagongshe.com/reaction/387315

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2,3-Dichloro-5,6-dicyano-1,4-benzoquinoneHCID 6775—
ReactantHCID 59332638HCID 59332638—
SolventChloroformHCID 6212—
ProductHCID 59332625HCID 59332625—

Reaction Steps

DDQ (17 mg, 0.075 mmol) was added to a solution of 5-bromo-4-fluoro-2,3-dihydro-1H-indole-7-carboxylic acid (17 mg, 0.066 mmol) in CHCl3 (2 mL) at room temperature. The reaction was stirred for 5 h and filtered. The precipitate was washed with CHCl3, and the filtrate was evaporated, giving the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08372875B2
Source datasetuspto-grants-2013_02
ORD IDord-5f1d902aca3f4bf4a8ab86ae1bc60e8c
Source noteuspto-grants-2013_02