HRID387403
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
Benzyl azide (0.340 g, 2.55 mmol), 1-hexyne (0.580 ml, 5.05 mmol), Cp*RuCl(PPh3)2 (50 mg, 0.063 mmol). Solvent, benzene; reaction temperature, 80° C.; reaction time, 3 hours; yield, 0.45 g (82%). EI-MS: m/z 216 [M+1].
WORKUP
后处理
- customreaction temperature, 80° C.
- customreaction time, 3 hours
- customyield