HuagongsheHuagongshe Chemistry Print Report · For research reference only
phenyl N-(1,3-thiazol-2-yl)carbamate → HCID 58931002, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | phenyl N-(1,3-thiazol-2-yl)carbamate | HCID 651148 | — |
| Reactant | HCID 58931472 | HCID 58931472 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 58931002 | HCID 58931002 | 77.7% |
Reaction Steps
4-(6-(Pyridin-2-yl)-7H-pyrrolo[2,3-d]pyrimidin-4-yloxy)phenylamine (100 mg) and (thiazol-2-yl)carbamic acid phenyl ester (116 mg) were heated and stirred in dimethylsulfoxide (2.5 ml) at 80° C. for 1 hour, in the same manner as Example 224, to obtain the title compound (110 mg) as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08372981B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-4ba41eb2daa8448b9813605e14b6caf5 |
| Source note | uspto-grants-2013_02 |