Anisole → HCID 10321810, compound

HRID 388195Notes

Reaction equation

[F:1][P-:2]([F:7])([F:6])([F:5])([F:4])[F:3].CO[C:10]1[CH:15]=[CH:14][C:13]([I+:16][C:17]2[CH:22]=[CH:21][C:20]([O:23][CH3:24])=[CH:19][CH:18]=2)=[CH:12][CH:11]=1.C1(OC)C=CC=CC=1>>[F:1][P-:2]([F:7])([F:6])([F:5])([F:4])[F:3].[C:13]1([I+:16][C:17]2[CH:22]=[CH:21][C:20]([O:23][CH3:24])=[CH:19][CH:18]=2)[CH:12]=[CH:11][CH:10]=[CH:15][CH:14]=1

Participants

Reactant 2

HCID 7519Anisole

HCID 14008200HCID 14008200, compound

Product 1

HCID 10321810HCID 10321810, compound

Procedure

Phenyl-4-methoxyphenyliodonium hexafluorophosphate was synthesized according to the procedure described for the synthesis of bis(p-methoxyphenyl)iodonium hexafluorophosphate from the corresponding aryliodonium diacetate and anisole. (77.9%)

Sources & evidence

ORD record: ord-9d4dac0f379e477187a02a14f43ca968
Source dataset: uspto-grants-2013_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08377704B2

Reaction notes

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