HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Piperidone → HCID 57821257, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Piperidone | HCID 33721 | — |
| Reactant | Ethyl 2-(chloromethyl)-5-methyl-4-oxo-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxylate | HCID 2339310 | — |
| Product | HCID 57821257 | HCID 57821257 | — |
Reaction Steps
Using ethyl 2-chloromethyl-5-methyl-4-oxo-3,4-dihydrothieno-[2,3-d]pyrimidine-6-carboxylate and piperidin-4-one, a substitution reaction was carried out similarly to later appearing Production Example 21. Successively the reaction product was hydrolyzed similarly to Example 33, without intervening isolation of the reaction product, to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08377944B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-0746f51183fd4898883ea8539c3cf10f |
| Source note | uspto-grants-2013_02 |