HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorophenylboronic acid → HCID 58282664, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorophenylboronic acid | HCID 74299 | — |
| Reactant | HCID 58282711 | HCID 58282711 | — |
| Reactant | HCID 59533408 | HCID 59533408 | — |
| Product | HCID 58282664 | HCID 58282664 | 45% |
Reaction Steps
4-Methoxy-6-(4-chloro-phenyl)-2-(3-trifluoromethyl-pyrazol-1-yl)-pyrimidine 307e was synthesized from compound 305 (1 g, 3.59 mmol) and (4-chloro-phenyl)-boronic acid 306e (842 mg, 5.39 mmol), according to the procedure as described for compound 307b, was a beige solid in 45% yield. MS (ESI, EI+) m/z=355 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08377962B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-658120dd4c8c410398fe1b634b177a12 |
| Source note | uspto-grants-2013_02 |