HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13519461, compound → HCID 68940045, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13519461 | HCID 13519461 | — |
| Catalyst | Platinum | HCID 23939 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 68940045 | HCID 68940045 | — |
Reaction Steps
The compound of Example 15B (89 mg) was dissolved in acetic acid and hydrogenated over 10% platinum on carbon. After purging with nitrogen, the mixture was filtered through a pad of diatomaceous earth to remove catalyst and concentrated in vacuo to give material that was carried forward to the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08377913B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-edb4a6a0735c4ca89473a01c81a4d43f |
| Source note | uspto-grants-2013_02 |