HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 62683031, compound → HCID 63360593, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 62683031 | HCID 62683031 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 63360593 | HCID 63360593 | 112% |
Reaction Steps
10% palladium-carbon (containing 50% water, 500 mg) was added to a solution of N-ethyl-3-(methylamino)-4-nitrobenzamide (1.99 g) in ethanol (50 ml), followed by stirring at ambient pressure under a hydrogen atmosphere for 15 hours. The reaction solution was filtered with celite and the solvent was evaporated under reduced pressure to obtain 4-amino-N-ethyl-3-(methylamino)benzamide (1.93 g) as a light red-purple oily product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08377923B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-5e8abad73d9e43d98d4c837ce28bc11a |
| Source note | uspto-grants-2013_02 |