HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 389238Generated: October 31, 2026
1,4-Dichlorobenzene → HCID 14298267, compound
https://huagongshe.com/reaction/389238
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1,4-Dichlorobenzene | HCID 4685 | — |
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Benzothiazole, 2-methyl-6-nitro- | HCID 76250 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 14298267 | HCID 14298267 | — |
Reaction Steps
To 2-methyl-6-nitrobenzothiazole (0.36 g) was added ethyl iodide (1.5 ml) and dichlorobenzene (20 ml). The mixture was heated to 120° C. for 2 days and then allowed to cool to room temperature. Ethyl acetate was added and the resulting precipitate removed by filtration. Drying in a vacuum oven gave the desired material (80 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08378120B2 |
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| Source dataset | uspto-grants-2013_02 |
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| ORD ID | ord-96c1b9790d6748e79d838e18df049e74 |
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| Source note | uspto-grants-2013_02 |
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