Isobutyric Acid → HCID 21900164, compound

HRID 389349Notes

Reaction equation

HRID 389349 reaction equation
[OH-].[CH2:2]([N+:6]([CH2:15][CH2:16][CH2:17][CH3:18])([CH2:11][CH2:12][CH2:13][CH3:14])[CH2:7][CH2:8][CH2:9][CH3:10])[CH2:3][CH2:4][CH3:5].[C:19]([OH:24])(=[O:23])[CH:20]([CH3:22])[CH3:21]>O>[C:19]([O-:24])(=[O:23])[CH:20]([CH3:22])[CH3:21].[CH2:15]([N+:6]([CH2:2][CH2:3][CH2:4][CH3:5])([CH2:7][CH2:8][CH2:9][CH3:10])[CH2:11][CH2:12][CH2:13][CH3:14])[CH2:16][CH2:17][CH3:18]

Participants

4

Reactant 2

HCID 6590Isobutyric AcidHCID 2723671Tetrabutylammonium Hydroxide

Product 1

HCID 21900164HCID 21900164, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

A 40 wt % solution of tetrabutylammonium hydroxide in water (250 mL, 99 g, 382 mmol), water (300 mL) and isobutyric acid (33.8 g, 382 mmol) was stirred at ambient temperature for 30 min. The solvent was removed in vacuo to afford the title compound (5) as a waxy solid, which was used without further purification.

Workup

  1. customThe solvent was removed in vacuo

Sources & evidence

ORD record
ord-a29b252949c44db682a3450bd1fe989a
Source dataset
uspto-grants-2013_02
Patent number
US08378137B2

Reaction notes

Loading…