HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butylamine → N-{[7-(Methylsulfonyl)-3,4-dihydro-2H-chromen-2-YL]methyl}butan-1-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butylamine | HCID 8007 | — |
| Reactant | [7-(methylsulfonyl)-3,4-dihydro-2H-chromen-2-yl]methyl 4-methylbenzenesulfonate | HCID 86652940 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | N-{[7-(Methylsulfonyl)-3,4-dihydro-2H-chromen-2-YL]methyl}butan-1-amine | HCID 44468515 | — |
Reaction Steps
Preparation according to Example 25: [7-(methylsulfonyl)-3,4-dihydro-2H-chromen-2-yl]methyl 4-methylbenzenesulfonate (0.020 g, 0.0504 mmol), butan-1-amine (0.5 ml), ACN (3 ml). MS m/z (rel. intensity, 70 eV) 297 (M+, 6), 254 (9), 131 (8), 87 (7), 86 (bp), 77 (7).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08524766B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-6e4595910f8c4bae916cc332812ac131 |
| Source note | uspto-grants-2013_09 |