反应详情

A solution of 1 g of 4-(2-bromoacetyl)benzonitrile in acetonitrile (5 mL) and water (10 mL) is treated under microwave irradiation (125° C., 50 min). The same experiment is conducted five times. All the vials are collected, extracted with ethyl ether, dried over magnesium sulfate and concentrated under vacuum to give the desired compound.

1. customAll the vials are collected
2. extractionextracted with ethyl ether
3. dry with materialdried over magnesium sulfate
4. concentrationconcentrated under vacuum