反应详情

A solution of 776 mg of 3-(2-bromoacetyl)benzonitrile in acetonitrile (5 mL) and water (10 mL) is treated under microwave irradiation (125° C., 50 min). The same experiment is realized a second time with 976 mg. All the vials are collected, extracted with ethyl ether, dried over magnesium sulfate and concentrated under vacuum to give the desired compound.

1. customAll the vials are collected
2. extractionextracted with ethyl ether
3. dry with materialdried over magnesium sulfate
4. concentrationconcentrated under vacuum