HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → HCID 12366387, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | HCID 67441412 | HCID 67441412 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12366387 | HCID 12366387 | — |
Reaction Steps
To a solution of EXAMPLE 1D (778 mg, 2.58 mmol) in ethanol (10 mL) was added hydrazine (83 mg, 2.58 mmol) and the mixture was refluxed for 2 hours. After cooling, the precipitated solid was collected by filtration and dried under vacuum to yield the title compound. MS (ESI) m/z 316 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08383623B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-b86b2683ce9d4febae8f56342358b8ac |
| Source note | uspto-grants-2013_02 |