HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 44818367, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 58296328 | HCID 58296328 | — |
| Reactant | HCID 86654203 | HCID 86654203 | — |
| Product | HCID 44818367 | HCID 44818367 | — |
Reaction Steps
The product was prepared from 8-bromo-4-[(3-methylphenyl)amino]-2-(methylthio)pyrido[4,3-d]pyrimidin-5(6H)-one using mCPBA/1,1-dimethylethyl (3-aminopropyl)carbamate and TFA sequences similar that described for Example 1 (Scheme 2). It was purified using reverse-phase HPLC.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08383635B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-d2090a4d61df45ccb80ad80a30ebaa36 |
| Source note | uspto-grants-2013_02 |